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| 3. |  | SÁ, Í. P.; SOUZA, G. B. de; NOGUEIRA, A. R. de A. Especiação de Cr(VI) em fertilizantes orgânicos por meio da extração em ponto nuvem e otimização através do planejamento experimental Doehlert. In: ENCONTRO NACIONAL DE QUÍMICA ANALÍTICA, 19., 2018, Caldas Novas, GO; CONGRESSO IBEROAMERICANO DE QUÍMICA ANALÍTICA, 7., Caldas Novas, GO. Anais... Caldas Novas,GO: ENQA; CIAQA, 2018. p.667.| Biblioteca(s): Embrapa Pecuária Sudeste. |
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| 4. | | LANDGRAFF, R. L.; MARCANO DE HIGUERA, J.; SÁ, I. P. DE; NOGUEIRA, A. R. de A. Determinação de Al, Ba, Cd, Cr, Cu, Fe, Sr e Ti em velas do tipo estrela empregando planejamento Box-Behnken. In: JORNADA CIENTÍFICA DA EMBRAPA SÃO CARLOS, 12., 2020, São Carlos, SP. Anais... São Carlos, SP: Embrapa Instrumentação; Embrapa Pecuária Sudeste, 2020. p.52. (Embrapa Instrumentação. Documentos, 71).| Biblioteca(s): Embrapa Pecuária Sudeste. |
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| 5. | | MARCANO DE HIGUERA, J.; SÁ, I. P. DE; LANDGRAFF, R. L.; NOGUEIRA, A. R. de A. Determination of Al, Ba, Cd, Cr, Cu, Fe, Sr, and Ti in Sparkler Candles by MIP OES. Food Analytical Methods, p. 317-329, 2021.| Biblioteca(s): Embrapa Pecuária Sudeste. |
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| 7. | | SÁ, I. P.; BANHOS, S.; ANDRADE, M. S.; NHAMUE, P. F.; NOGUEIRA, A. R. de A. Chemical speciation of hexavalent chromium in organic fertilizer by LC-ICP-MS and spectrophotometry. In: BRAZILIAN MEETING ON CHEMICAL SPECIATION, 7.; RIO SYMPOSIUM ON ATOMIC SPECTROMETRY, 16., 2023, Bento Gonçalves, RS. Abstracts... 2023.| Biblioteca(s): Embrapa Pecuária Sudeste. |
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| 12. | | COELHO, T. L. S.; SILVA, D. S. N.; SOUZA FILHO, L. B. DE; ROCHA, J. M.; MARCANO DE HIGUERA, J.; SÁ, I. P. DE; GAMELA, R. R.; NOGUEIRA, A. R. de A.; LOPES JÚNIOR, C. A.; VIEIRA, E. C. High enhancement of macro and micronutrients quantification in Cajuína by ICP OES using ultrasound and multivariate analysis. Food Chemistry Advances, v. 2, 2023. 8 p.| Biblioteca(s): Embrapa Pecuária Sudeste. |
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| 13. | | SILVA, F. L. F. da; ANDRADE NETO, D. M.; MENEZES, F. L. de; SÁ, I. P. de; MARCANO DE HIGUERA, J.; FECHINE, P. B. A; COSTA, L. S. da; NOGUEIRA, A. R. de A.; LOPES. G. S; MATOS, W. O. Non-chromatographic arsenic speciation analyses in wild shrimp (Farfantepenaeus brasiliensis) using functionalized magnetic iron-nanoparticles. Food Chemistry, v.345, 2021, 128781. 9 p.| Biblioteca(s): Embrapa Pecuária Sudeste. |
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 | Acesso ao texto completo restrito à biblioteca da Embrapa Pecuária Sudeste. Para informações adicionais entre em contato com cppse.biblioteca@embrapa.br. |
Registro Completo
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Biblioteca(s): |
Embrapa Pecuária Sudeste. |
|
Data corrente: |
07/07/2021 |
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Data da última atualização: |
28/09/2021 |
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Tipo da produção científica: |
Artigo em Periódico Indexado |
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Circulação/Nível: |
A - 2 |
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Autoria: |
SILVA, A. B. S. do; SÁ, I. P. de; MARCANO DE HIGUERA, J.; NOGUEIRA, A. R. de A. |
|
Afiliação: |
ANA BEATRIZ SANTOS DA SILVA, UFSCAR; ÍVERO PITA DE SÁ, UFSCAR; JULYMAR MARCANO DE HIGUERA, UFSCAR; ANA RITA DE ARAUJO NOGUEIRA, CPPSE. |
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Título: |
Feasibility of dispersive liquid-liquid microextraction for molybdenum determination in lamb meat by MIP OES. |
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Ano de publicação: |
2021 |
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Fonte/Imprenta: |
Food Analytical Methods, v.14, 2021. |
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Páginas: |
p.496-502. |
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ISSN: |
1936-976X |
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DOI: |
https://doi.org/10.1007/s12161-020-01898-x |
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Idioma: |
Inglês |
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Conteúdo: |
The dispersive liquid?liquid microextraction (DLLME) was evaluated as a strategy to improve the MIP OES sensitivity for molybdenum determination in lamb meat. Initially, the dispersive (methanol) and extracting (tetrachloromethane) solvents were selected based on a mixture design. The best results were achieved with methanol and carbon tetrachloride as dispersive and extracting solvent, respectively. The operational parameters, such as pH, volume of dispersive and extractant solvents, and complexing agent concentration (8-hydroxyquinoline) were optimized using a Box-Behnken design. The optimal conditions were established as pH 3.8, 90 uL of carbon tetrachloride, 480 uL of methanol, and 1.09 mmol L-1 of 8-hydroxyquinoline. Besides, the use of external gas module control (EGCM) was explored to minimize the matrix effects caused by the organic solvent introduction. The accuracy of the proposed method was estimated employing a certificate reference material (bovine liver, NIST 1577c) and the obtained recovery was 92%. The limit of detection was found to be 0.20 ug g-1, and the enrichment factor was 4.5. The DLLME-MIP OES was applied for six samples of lamb meat, and the results compared to ICP-MS presented no statistical difference. Therefore, the proposed method showed satisfactory accuracy and suitable sensitivity. |
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Palavras-Chave: |
DLLME; MIP OES; Sample preparation; Trace analysis. |
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Thesaurus NAL: |
Microextraction. |
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Categoria do assunto: |
W Química e Física |
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Marc: |
LEADER 02099naa a2200253 a 4500
001 2132839
005 2021-09-28
008 2021 bl uuuu u00u1 u #d
022 $a1936-976X
024 7 $ahttps://doi.org/10.1007/s12161-020-01898-x$2DOI
100 1 $aSILVA, A. B. S. do
245 $aFeasibility of dispersive liquid-liquid microextraction for molybdenum determination in lamb meat by MIP OES.$h[electronic resource]
260 $c2021
300 $ap.496-502.
520 $aThe dispersive liquid?liquid microextraction (DLLME) was evaluated as a strategy to improve the MIP OES sensitivity for molybdenum determination in lamb meat. Initially, the dispersive (methanol) and extracting (tetrachloromethane) solvents were selected based on a mixture design. The best results were achieved with methanol and carbon tetrachloride as dispersive and extracting solvent, respectively. The operational parameters, such as pH, volume of dispersive and extractant solvents, and complexing agent concentration (8-hydroxyquinoline) were optimized using a Box-Behnken design. The optimal conditions were established as pH 3.8, 90 uL of carbon tetrachloride, 480 uL of methanol, and 1.09 mmol L-1 of 8-hydroxyquinoline. Besides, the use of external gas module control (EGCM) was explored to minimize the matrix effects caused by the organic solvent introduction. The accuracy of the proposed method was estimated employing a certificate reference material (bovine liver, NIST 1577c) and the obtained recovery was 92%. The limit of detection was found to be 0.20 ug g-1, and the enrichment factor was 4.5. The DLLME-MIP OES was applied for six samples of lamb meat, and the results compared to ICP-MS presented no statistical difference. Therefore, the proposed method showed satisfactory accuracy and suitable sensitivity.
650 $aMicroextraction
653 $aDLLME
653 $aMIP OES
653 $aSample preparation
653 $aTrace analysis
700 1 $aSÁ, I. P. de
700 1 $aMARCANO DE HIGUERA, J.
700 1 $aNOGUEIRA, A. R. de A.
773 $tFood Analytical Methods$gv.14, 2021.
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